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[ CAS No. 7292-74-2 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 7292-74-2
Chemical Structure| 7292-74-2
Structure of 7292-74-2 * Storage: {[proInfo.prStorage]}

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Product Details of [ 7292-74-2 ]

CAS No. :7292-74-2 MDL No. :MFCD00049325
Formula : C8H8FNO2 Boiling Point : No data available
Linear Structure Formula :- InChI Key :LVYBCZIDQKJNFP-UHFFFAOYSA-N
M.W : 169.15 Pubchem ID :265434
Synonyms :
Chemical Name :2-Amino-2-(3-fluorophenyl)acetic acid

Safety of [ 7292-74-2 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 7292-74-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7292-74-2 ]

[ 7292-74-2 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 24424-99-5 ]
  • [ 7292-74-2 ]
  • [ 142121-94-6 ]
YieldReaction ConditionsOperation in experiment
69% To a suspension of <strong>[7292-74-2]2-amino-2-(3-fluorophenyl)acetic acid</strong> (1.00 g, 5.91 mmol) in THF (30 ml) and water (30 ml), 2N sodium hydroxide (29.6 ml, 59.1 mmol) and di-tert-butyl dicarbonate (2.58 g, 1 1.8 mmol) were added and the reaction was stirred at RT for 15h. THF was evaporated, the aqueous phase was cooled and acidified with 37% HCl until pH 1. The desired compound was extracted with EtOAc and the organic phase was washed with brine, dried over Na2SO4 and evaporated to obtain 2-(tert-butoxycarbonylamino)-2-(3- fluorophenyl)acetic acid (1.10 g; 69% yield).
69% With sodium hydroxide; In tetrahydrofuran; water; at 20℃; for 15h; To a suspension of <strong>[7292-74-2]2-amino-2-(3-fluorophenyl)acetic acid</strong> (1.00 g, 5.91 mmol) in THF (30 ml) and water (30 ml), were added 2N sodium hydroxide (29.6 ml, 59.1 mmol) and di-tert-butyl dicarbonate (2.58 g, 11.8 mmol), and the reaction was stirred at RT for 15 hours. THF was evaporated, and the aqueous phase was cooled and acidified with 37% HCl until pH 1. The desired compound was extracted with EtOAc, and the organic phase was washed with brine, dried over Na2SO4 and evaporated to obtain 2-(tert-butoxycarbonylamino)-2-(3-fluorophenyl)acetic acid (1.10 g; 69% yield).
  • 2
  • (3-Fluoro-phenyl)-[(E)-hydroxyimino]-acetic acid [ No CAS ]
  • [ 7292-74-2 ]
  • 3
  • [ 271583-22-3 ]
  • [ 7292-74-2 ]
YieldReaction ConditionsOperation in experiment
Substitution in the procedure of Example 3 for the N-tert.-butoxycarbonyl derivative of D-α-aminophenylacetic acid (also called D-α-tert.-butoxycarboxamidophenylacetic acid) of an equimolar weight of the N-tert.-butoxycarbonyl derivative of ... D-α-amino-m-methylphenylacetic acid, D-α-amino-p-chlorophenylacetic acid, D-α-amino-m-chlorophenylacetic acid, D-α-amino-p-fluorophenylacetic acid, D-α-amino-m-fluorophenylacetic acid, D-α-amino-p-aminophenylacetic acid, D-α-amino-p-dimethylaminophenylacetic acid, D-α-amino-m,p-dimethoxyphenylacetic acid, ...
The hydantoin was hydrolyzed at reflux using 1 N NaOH giving 2-amino-2-(3-fluorophenyl)acetic acid which was esterified via Procedure H in methanol to give the title compound.
  • 5
  • [ 271583-58-5 ]
  • [ 7292-74-2 ]
  • 6
  • [ 271583-37-0 ]
  • [ 7292-74-2 ]
  • 7
  • [ 456-48-4 ]
  • [ 7292-74-2 ]
  • 8
  • [ 501-00-8 ]
  • [ 7292-74-2 ]
  • 9
  • [ 7292-74-2 ]
  • (R)-1-[2-tert-Butoxycarbonylamino-2-(3-fluoro-phenyl)-acetyl]-pyrrolidine-2-carboxylic acid [ No CAS ]
  • 10
  • [ 7292-74-2 ]
  • C20H17Cl3FNO6 [ No CAS ]
  • 11
  • [ 7292-74-2 ]
  • C32H41FN6O7 [ No CAS ]
  • 12
  • [ 7292-74-2 ]
  • [2-{(S)-2-[(S)-1-(Benzyloxycarbonylamino-imino-methyl)-2-oxo-piperidin-3-ylcarbamoyl]-pyrrolidin-1-yl}-1-(3-fluoro-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester [ No CAS ]
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