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CAS No. : | 70049-77-3 | MDL No. : | MFCD08063955 |
Formula : | C7H5Cl2NO3S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | SCYSJFKWFQZRJW-UHFFFAOYSA-N |
M.W : | 254.09 | Pubchem ID : | 3017979 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P260-P261-P264-P270-P271-P280-P301+P312-P301+P330+P331-P302+P352-P303+P361+P353-P304+P340-P305+P351+P338-P310-P312-P321-P322-P330-P363-P405-P501 | UN#: | 3261 |
Hazard Statements: | H302-H312-H314-H332 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In methanol; aluminium trichloride; | EXAMPLE 5 3-(4-Chloro-3-sulfamoylbenzoyl)-<strong>[4265-25-2]2-methylbenzo[b]furan</strong> is obtained as described in Example 1 from 10.1 g 4-chloro-3-sulfamoylbenzoyl chloride and 5.8 g <strong>[4265-25-2]2-methylbenzo[b]furan</strong> in the presence of 11.4 g aluminum chloride. After evaporation of the extraction agent, the residue is stirred with di-isopropyl ether, and the solids are filtered off. Colorless crystals, m.p. 183 C. (from methanol). |
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