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CAS No. : | 6950-43-2 | MDL No. : | MFCD00093013 |
Formula : | C7H4BrNO4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | FNINYRSNPGPWEL-UHFFFAOYSA-N |
M.W : | 246.02 | Pubchem ID : | 248528 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79.7% | With potassium permanganate; In water; at 50℃; | a 21.6g (0.1mol) of 2-nitro-nitration step to give 5-bromo-toluene was added 100mL of water was added with stirringand heated to 50 , 800g 5wt% was added potassium permanganate (0.253 mol) solution, the reaction incubated , the precipitate was removed by filtration, the filtrate wasadjusted with hydrochloric acid 1 + l pH<1 the precipitate was collected and dried to give 2-nitro-5-bromo - acid 19.6g (0.0797mol), a yield of79.7%, |
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