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[ CAS No. 68781-13-5 ] {[proInfo.proName]}

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Chemical Structure| 68781-13-5
Chemical Structure| 68781-13-5
Structure of 68781-13-5 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 68781-13-5 ]

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Product Details of [ 68781-13-5 ]

CAS No. :68781-13-5 MDL No. :MFCD00012545
Formula : C4H8ClNO2 Boiling Point : No data available
Linear Structure Formula :- InChI Key :WTZRHZRMLYNBRM-UHFFFAOYSA-N
M.W : 137.56 Pubchem ID :11957445
Synonyms :
Chemical Name :1-Aminocyclopropanecarboxylic acid hydrochloride

Safety of [ 68781-13-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 68781-13-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68781-13-5 ]

[ 68781-13-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6914-71-2 ]
  • [ 68781-13-5 ]
YieldReaction ConditionsOperation in experiment
58% With ammonia; In methanol; for 0.25h;Inert atmosphere; After reducing pressure in the reaction vessel, the vessel was filled with nitrogen gas, to which 6.8 ml of 7 NNH3 3 in MeOH was loaded. 1.0 g (6.30 mmol) of dimethylcyclopropane-1,1-dicarboxylate was dissolved in 63 ml ofMeOH, which was also loaded into the reaction vessel. If the starting material still remained, NH3 gas could be providedfor bubbling for 15 minutes. Upon completion of the reaction, the reaction solvent was eliminated by evaporation underreduced pressure and the precipitated solid compound was filtered and washed with 0°C methanol, followed by vacuumdrying. The obtained reaction product was dissolved in 5 ml of 7.4percent NaOH/H2O, followed by stirring at 40°C for 20minutes. Then, the temperature was lowered to room temperature (Reactant A). 7 ml of 12.3percent NaOCl and 2 ml of 30percentNaOH/H2O were stirred together at room temperature for 1 hour (Reactant B). These reactants A and B were mixedand stirred at 80°C for 4 minutes. After lowering the temperature thereof, 4 ml of hydrochloric acid was slowly addedthereto carefully not to increase the temperature more than 60°C. The solvent was eliminated by evaporation underreduced pressure and the reactant was dissolved in ethanol. The precipitated solid compound was filtered. The remainingsolution was evaporated under reduced pressure and then dissolved in hot acetone. The generated solid compoundwas filtered and dried to give 0.5 g of 1-aminocyclopropyl acetic acid hydrochloride (yield: 58percent).1H NMR (400 MHz, D2O delta 1.40-1.43 (m, 2H), 1.22-1.25 (m, 2H)
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