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CAS No. : | 6451-86-1 | MDL No. : | MFCD00666893 |
Formula : | C15H13BrO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | RUBXMEDWBCBLEZ-UHFFFAOYSA-N |
M.W : | 321.17 | Pubchem ID : | 10903319 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
95.3% | In 1,4-dioxane; acetic acid; at 20℃; | 24 g to oxybenzylphenyl ethanol, 35 g 2 - bromo -5 - benzyloxy -4 - methoxy benzaldehyde and 10 g of methyl amine hydrochloride dispersed dissolved in 300 ml 1, 4 - dioxane, 30 g sodium dissolved in 10 ml acetic acid in, under the room temperature condition in the solution into the raw materials, the reaction at room temperature, HPLC monitoring reaction to the raw material of the basic reaction is complete, water quenching reaction, for 500 ml methylene chloride and 200 ml water extraction, in the organic phase, to obtain N - methyl - (4 - oxybenzylphenyl ethyl) -2 - bromo -5 - benzyloxy -4 - methoxybenzylamine cyano boron hydrogenated compound of the dichloromethane solution, measured by HPLC in this solution - N - methyl (4 - oxybenzylphenyl ethyl) -2 - bromo -5 - benzyloxy -4 - methoxybenzylamine cyano boron hydrogenated compound has a purity of 95.3percent. |
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