[ CAS No. 611-79-0 ] {[proInfo.proName]}

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2D 3D

Structure of 611-79-0 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 611-79-0 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 611-79-0 ]

SDS Specification

Alternatived Products of [ 611-79-0 ]

Product Details of [ 611-79-0 ]

CAS No. :	611-79-0	MDL No. :	MFCD00014774
Formula :	C₁₃H₁₂N₂O	Boiling Point :	No data available
Linear Structure Formula :	-	InChI Key :	TUQQUUXMCKXGDI-UHFFFAOYSA-N
M.W :	212.25	Pubchem ID :	69145
Synonyms :

Safety of [ 611-79-0 ]

Signal Word:	Warning	Class:
Precautionary Statements:	P261-P305+P351+P338	UN#:
Hazard Statements:	H315-H319-H335	Packing Group:
GHS Pictogram:

Application In Synthesis of [ 611-79-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 611-79-0 ]

[ 611-79-0 ] Synthesis Path-Downstream 1~1

1
[ 25032-74-0 ]
[ 611-79-0 ]
C₃₉H₂₄N₂O₃ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
10.6%	With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 100℃; for 24h;	A catalyst consisting of tris(dibenzylideneacetone)-dipalladium(0) (Pd2dba3) (2.747 g, 3 mmol) and tris(tert-butyl)phosphine (18.2 mL, 18 mmol) dissolved in 100 mL toluene and preformed by stirring for 15 min at room temperature was added to <strong>[25032-74-0]bis(3-bromophenyl)methanone</strong> (20.4006 g, 60 mmol), bis(3-aminophenyl)methanone (6.3675 g, 30 mmol), and sodium tert-butoxide (17.298 g, 180 mmol) dissolved in 400 mL toluene. This mixture was stirred for 24 h at 100 C and then cooled to room temperature, filtered off, and washed with CH2Cl2. After removing the solvent, the product was purified by chromatography on silica gel with petroleum ether/CH2Cl2 as eluent and recrystallized from tetrahydrofuran/methanol to obtain the desired pure product (yield = 1.81 g, 10.6%). 1H NMR (500 MHz, CDCl3): δ 7.66 (dt, J = 7.6 Hz, 1.3 Hz, 6H), 7.44 (t, J = 7.8 Hz, 6H), 7.37 (ddd, J = 8.0 Hz, 2.1 Hz, 1.1 Hz, 6H), 6.92 (t, J = 1.8 Hz, 6H). 13C NMR (126 MHz, CDCl3): δ 194.94, 148.99, 138.10, 131.04, 130.92, 129.20, 125.70. Anal. calcd (%) for C39H24N2O3: C 82.38, H 4.25, N 4.93; found: C 82.21, H 4.19, N 4.98. APCI-MS (m/z): [M]+ calculated for C39H24N2O3, 568.63; found, 569.5.

Reference： [1]Chinese Chemical Letters,2021,vol. 32,p. 1017 - 1019

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Technical Information

? Baeyer-Villiger Oxidation ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Benzylic Oxidation ? Birch Reduction ? Blanc Chloromethylation ? Bucherer-Bergs Reaction ? Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions ? Chan-Lam Coupling Reaction ? Clemmensen Reduction ? Corey-Bakshi-Shibata (CBS) Reduction ? Corey-Chaykovsky Reaction ? Fischer Indole Synthesis ? Friedel-Crafts Reaction ? Grignard Reaction ? Henry Nitroaldol Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Hydrogenolysis of Benzyl Ether ? Lawesson's Reagent ? Leuckart-Wallach Reaction ? Mannich Reaction ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Peterson Olefination ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Aldehydes and Ketones ? Preparation of Alkylbenzene ? Preparation of Amines ? Prins Reaction ? Reactions of Aldehydes and Ketones ? Reactions of Amines ? Reactions of Benzene and Substituted Benzenes ? Reformatsky Reaction ? Robinson Annulation ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Specialized Acylation Reagents-Ketenes ? Specialized Acylation Reagents-Vilsmeier Reagent ? Stobbe Condensation ? Tebbe Olefination ? Ugi Reaction ? Vilsmeier-Haack Reaction ? Wittig Reaction ? Wolff-Kishner Reduction

Historical Records

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[ 611-79-0 ]

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P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
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P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
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P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P402 + P404	Store in a dry place. Store in a closed container.
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P411 + P235	Keep cool.
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P501	Dispose of contents/container to ...
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Physical hazards
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H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
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H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
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H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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[ CAS No. 611-79-0 ] {[proInfo.proName]}

Quality Control of [ 611-79-0 ]

Related Doc. of [ 611-79-0 ]

Product Details of [ 611-79-0 ]

Safety of [ 611-79-0 ]

Application In Synthesis of [ 611-79-0 ]

[ 611-79-0 ] Synthesis Path-Downstream 1~1

Technical Information

Related Functional Groups of [ 611-79-0 ]

Aryls

Ketones

Amines

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Related Functional Groups of
[ 611-79-0 ]