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CAS No. : | 5159-41-1 | MDL No. : | MFCD00004610 |
Formula : | C7H7IO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | WZCXOBMFBKSSFA-UHFFFAOYSA-N |
M.W : | 234.03 | Pubchem ID : | 107629 |
Synonyms : |
|
Chemical Name : | 2-Iodobenzyl alcohol |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
21% | General procedure: To a suspension of NaH (60% dispersion in oil, 297 mg) in THF (7 mL), was added a solution of o-iodobenzyl alcohol (1,4 g, 6.0 mmol) in THF (12 mL). Effervescence occurred and the mixture was stirred at room temperature for 20 min. A solution of the arylsulfonyl chloride (9.0 mmol) in THF (10 mL) was added and the mixture stirred for 24 h. Water (30 mL) was added and the mixture extracted with ether (3 x 25 mL), dried (MgSO4) and the solvent evaporated. The residue was purified by column chromatography or crystallisation. |
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