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CAS No. : | 50910-54-8 | MDL No. : | MFCD00012566 |
Formula : | C6H14ClNO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 151.63 | Pubchem ID : | - |
Synonyms : |
|
Chemical Name : | trans-4-Aminocyclohexanol hydrochloride |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
81% | With potassium carbonate; In water; at 20℃; for 1h; | 12A: 2-((/ra?^)-4-Hydroxycyclohexyl)isoindoline~l ,3H -dione[00150] A mixture of (irans)-4-aminocyclohexanol, HC1 (5 g, 33.0 mmol) and ethyl l,3-dioxoisoindoline-2-carboxylate (7.23 g, 33.0 mmol) in water (50 mL) was treated with K2C03 (11.39 g, 82 mmol) and stirred at room temperature for 1 h. The mixture became very viscous, more water (50 mL) was added and it was stirred for another 2 h. The white solid was collected by filtration, washed with water, and air- dried to provide 12A (6.52g, 81 % yield). 1H NMR (400 MHz, DMSO-d6) δ ppm 7.66-7.84(m, 4H); 4.56(br. s, 1H); 3.79-3.93(m, 1H); 3.29-3.45(m, 1H); 1.97-2.14(m, 2H); 1.76- L91(m, 2H); 1.50-1.67(m, 2H); 1.09-1.28(m, 2H). |
With potassium carbonate; In water; at 20℃; for 3h; | N-Ethoxycarbonylphthalimide (10Og; 0.46 mol) was added to a mixture of trans-4- hydroxycyclohexylamine hydrochloride (69 g; 0.46 mol), potassium carbonate (158 g; 1.15 mol) and water (1 L) at room temperature. After stirring for 3h the title compound (95 g) was isolated by filtration, washing with water then ethyl acetate,. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Trans-4-aminocyclohexanol hydrochloride (500 mg) was dissolved DMF (11 mL) prior to the addition of <strong>[17794-48-8](3-trifluoromethyl-benzoylamino)-acetic acid</strong> (815.0 mg) and 4-methylmorpholine (1.0 mL). After 5 min, BOP reagent (1.4 g) was added and the reaction was stirred overnight. Ethyl acetate was added, and the solution was washed with brine, 1N HCl, and saturated NaHCO3. The desired (trans)-N-[(4-hydroxy-cyclohexylcarbamoyl)-methyl]-3-trifluoromethyl-benzamide (480.5 mg) was then collected as a solid. MS found: (M+H)+=345.1. |
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