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[ CAS No. 4848-43-5 ] {[proInfo.proName]}

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Chemical Structure| 4848-43-5
Chemical Structure| 4848-43-5
Structure of 4848-43-5 * Storage: {[proInfo.prStorage]}

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Product Details of [ 4848-43-5 ]

CAS No. :4848-43-5 MDL No. :MFCD00233831
Formula : C14H16NP Boiling Point : -
Linear Structure Formula :(C6H5)2P(CH2)2NH2 InChI Key :RXEPBCWNHKZECN-UHFFFAOYSA-N
M.W : 229.26 Pubchem ID :273264
Synonyms :

Safety of [ 4848-43-5 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:2735
Hazard Statements:H314 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 4848-43-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4848-43-5 ]

[ 4848-43-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 53400-41-2 ]
  • [ 4848-43-5 ]
  • N-[2-(diphenylphosphanyl)ethyl]-5,6,7,8-tetrahydroquinolin-8-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 33℃; for 6h;Inert atmosphere; N2 protection,1.47 g (10 mmol) of 5,6,7,8-tetrahydroquinolinone was added to a 250 ml round bottom flask,Then, 3 g (13.2 mmol) of 2- (diphenylphosphino) ethylamine and 4.43 g (21 mmol)Of sodium triacetoxyborohydride. Add 100 ml of DCE solvent,The solution was pale yellow emulsion, stirred at 33 C for 6 h, the reaction solution was quenched with saturated NaHCO3 solution,Diluted with water, extracted with ethyl acetate (3X30ml). The extract was dried over anhydrous sodium sulfate and spin dried to give 3.32 g of crude product. With ethyl acetate: petroleum ether = 1: 10 had a column of yellow oil as pure,Yield: 75%;
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