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CAS No. : | 4774-34-9 | MDL No. : | MFCD00087111 |
Formula : | C5H3N3O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | SVOQOFSQLVVHKQ-UHFFFAOYSA-N |
M.W : | 121.10 | Pubchem ID : | 12210265 |
Synonyms : |
|
Signal Word: | Danger | Class: | N/A |
Precautionary Statements: | P280-P301+P312+P330-P305+P351+P338+P310 | UN#: | N/A |
Hazard Statements: | H302-H318 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With phosphorus pentachloride; trichlorophosphate;N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile; | EXAMPLE 76 4-(1,2,4,5-Tetrahydro-benzo[d]azepin-3-yl)-pyrimidine-5-carbonitrile In analogy to the procedure described in example 4 the 4-chloro-pyrimidine-5-carbonitrile (prepared from <strong>[4774-34-9]4-hydroxy-5-pyrimidine-carbonitrile</strong> and phosphorus oxychloride, phosphorus pentachloride and N-ethyl-N,N-diisopropylamine in acetonitril at reflux) was treated with 2,3,4,5-tetrahydro-1H-benzo[d]azepine hydrochloride [J. Heterocycl. Chem. (1971), 8(5), 779-83] in N,N-dimethylformamide in the presence of N-ethyl-N,N-diisopropylamine at room temperature to yield the 4-(1,2,4,5-tetrahydro-benzo[d]azepin-3-yl)-pyrimidine-5-carbonitrile as off white solid; MS: [M+H]+=251; m.p. 148-150 C. |
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