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CAS No. : | 473416-12-5 | MDL No. : | MFCD07371609 |
Formula : | C9H8N2O2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | LPLOEZPPYOSNEW-UHFFFAOYSA-N |
M.W : | 176.17 | Pubchem ID : | 22260640 |
Synonyms : |
|
Chemical Name : | Methyl 1H-indazole-5-carboxylate |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
80% | With N-Bromosuccinimide; In tetrahydrofuran; at 20℃; | A mixture of compound 1 (1.7 g, 0.01 mol) and NBS (2.1 g, 0.012 mol) in THF (10 ml) was stirred at r.t. overnight. The mixture was concentrated to yield a residue, to which was added DCM (5 ml). After stirring for 30 min, the solution was filtered to yield compound 2 (1.9 g, 80%) as a light yellow solid. |
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