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[ CAS No. 4316-53-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 4316-53-4
Chemical Structure| 4316-53-4
Structure of 4316-53-4 * Storage: {[proInfo.prStorage]}

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Product Details of [ 4316-53-4 ]

CAS No. :4316-53-4 MDL No. :MFCD03093256
Formula : C19H17N Boiling Point : -
Linear Structure Formula :(C6H5)2NC6H4CH3 InChI Key :IULUNTXBHHKFFR-UHFFFAOYSA-N
M.W : 259.35 Pubchem ID :11299928
Synonyms :

Safety of [ 4316-53-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 4316-53-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4316-53-4 ]

[ 4316-53-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 4316-51-2 ]
  • [ 75-24-1 ]
  • [ 4316-53-4 ]
YieldReaction ConditionsOperation in experiment
87% With bis(1,5-cyclooctadiene)nickel (0); sodium t-butanolate; 1,3-bis(cyclohexyl)imidazolium tetrafluoroborate; In toluene; at 100℃; for 6h;Sealed tube; Glovebox; Inert atmosphere; General procedure: Ni(cod)2 (3.4 mg, 0.025 mmol), ICy·HBF4 (4.0 mg, 0.025 mmol), NaOtBu (48 mg, 0.50 mmol) and toluene (0.50 mL) were added to a 10 mL-sample vial with a Teflon-sealed screwcap in a glovebox filled with nitrogen. The resulting mixture was stirred at room temperature for 3 min. An aryl methyl ether (0.25 mmol) in toluene (0.50 mL) and AlMe3 (1.8 M in toluene solution, 0.14 mL, 0.25 mmol) were then added to the vial and the screw cap was closed. The contents of the vial were stirred at 80 C for 6 or 18 h. The reaction mixture was cooled to room temperature, and the crude mixture was then treated with EtOH. The resulting mixture was filtered through a pad of silica gel, and then analyzed by GC. The filtrate was concentrated in vacuo to give a residue, which was purified by flash column chromatography over silica gel.
  • 2
  • [ 4316-53-4 ]
  • C38H32N2 [ No CAS ]
  • [ 65181-78-4 ]
  • N,N,N',N'-tetraphenyl-(2,2'-dimethyl)-(1,1'-biphenyl)-4,4'-diamine [ No CAS ]
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