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CAS No. : | 3891-07-4 | MDL No. : | MFCD00005903 |
Formula : | C10H9NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | MWFLUYFYHANMCM-UHFFFAOYSA-N |
M.W : | 191.18 | Pubchem ID : | 77499 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
24% | With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 80℃; for 5.5h; | 8 g (42.2 mmol) 2-chloro-4-fluoro-5-nitro toluene 31 are dissolved in DMF, treated with 8.07 g (42.2 mmol) N- (2-hydroxyethyl) phthalimide and 27.5 g (84.4 mmol) cesium carbonate and stirred for 5.5 h at 80 C. Then, the reaction mixture was cooled to room temperature. After customary workup, 3.65 g (24 %) of the substitution product is obtained as a pale yellow solid. |
24% | With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 50℃; for 5.5h; | 8 g (42.2 mmol) 2-Chloro-4-fluoro-5-nitrotoluene are dissolved in DMF, treated with 8.07 g (42.2 mmol) N- (2-Hydroxyethyl) phthalimide and 27.5 g (84.4 mmol) cesium carbonate and stirred at 80 C for 5.5 h. The reaction mixture is cooled to room temperature, filtered by suction and washed with DMF. The filtrate is evaporated to dryness. The residue is taken up in ethyl acetate, washed 3x with water and 1x with brine, dried over Na2SO4, filtered and evaporated. The residue is digested with diethylether/MTB-ether (1: 1), filtered by suction, washed with ethyl acetate/MTB-ether (1: 1) and dried in vacuo. Yield : 3.65 g (24 %), pale yellow solid |
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