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CAS No. : | 31558-41-5 | MDL No. : | MFCD00156964 |
Formula : | C9H9BrO3 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | BIFWGDWGCZLCHF-UHFFFAOYSA-N |
M.W : | 245.07 | Pubchem ID : | 777997 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
35% | With dimethyl sulfide borane; In chlorobenzene; at 0 - 130℃; for 21h;Inert atmosphere; | 4-Bromo-2,5-dimethoxybenzaldehyde (0.50 g, 2 mmol) was suspended in chlorobenzene (4 ml) and cooled to 0 C. Borane dimethylsulfide (0.60 ml, 6 mmol) was added with vigorous stirring, when effervescence ceased reaction mixture was heated for 3 h at 80 C and then for a further 18 h at 130 C. The reaction mixture was then quenched with sodium carbonate. The crude product was extracted into CH2Cl2, dried with magnesium sulfate and solvent removed in vacuo. This gave the product as a white solid: 1.03 g (35%); mp 88-90 C; 1H NMR (400 MHz, CDCl3) delta ppm 6.98 (s, 1H, ArH), 6.73 (s, 1H, ArH), 3.82 (s, 3H, OCH3), 3.76 (s, 3H, OCH3), 2.17 (s, 3H, CH3). |
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