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[ CAS No. 30389-33-4 ] {[proInfo.proName]}

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Chemical Structure| 30389-33-4
Chemical Structure| 30389-33-4
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Product Details of [ 30389-33-4 ]

CAS No. :30389-33-4 MDL No. :MFCD01862194
Formula : C9H9NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :UTTJAIFHRUAFED-UHFFFAOYSA-N
M.W : 163.17 Pubchem ID :169153
Synonyms :

Safety of [ 30389-33-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 30389-33-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 30389-33-4 ]

[ 30389-33-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 30389-33-4 ]
  • [ 1196155-38-0 ]
  • 5-((4-(aminomethyl)-6-(trifluoromethyl)pyridin-2-yl)oxy)-3,4-dihydroquinolin-2(1H)-one [ No CAS ]
  • 2
  • [ 30389-33-4 ]
  • [ 1196155-38-0 ]
  • 2-((2-oxo-1,2,3,4-tetrahydroquinolin-5-yl)oxy)-6-(trifluoromethyl)isonicotinonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
49% With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 20℃; for 3h; To a stirred solution of 5-hydroxy-3,4-dihydroquinolin-2(lH)-one 1 (50 mg, 0.31 mmol) in N-methyl-2-pyrrolidone (3 mL) at RT, were added 2-chloro-6- (trifluoromethyl)isonicotinonitrile (63 mg, 0.31 mmol) and K2C03 (85 mg, 0.61 mmol). The mixture was stirred at RT for 3 h. The mixture was diluted with water (10 mL) and extracted with EtOAC (2 x 15 mL). The combined organic extracts were washed with brine (10 mL), dried (Na2S04), filtered, and concentrated under reduced pressure. The crude was triturated with Et20 (2 x 5 mL) to afford compound 2 (50 mg, 49percent) as white solid. 1H NMR (400 MHz, OMSO-d6): delta 10.28 (s, 1H), 8.18 (s, 1H), 7.97 (s, 1H), 7.23 (t, J= 8.0 Hz, 1H), 6.85-6.78 (m, 2H), 2.65 (t, J = 7.6 Hz, 2H), 2.42-2.35 (m, 2H); LC-MS (ESI): m/z 332.1 (M - 1).
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Technical Information

? Acyl Group Substitution ? Appel Reaction ? Baeyer-Villiger Oxidation ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Bucherer-Bergs Reaction ? Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions ? Chan-Lam Coupling Reaction ? Chugaev Reaction ? Clemmensen Reduction ? Complex Metal Hydride Reductions ? Corey-Bakshi-Shibata (CBS) Reduction ? Corey-Chaykovsky Reaction ? Corey-Kim Oxidation ? Dess-Martin Oxidation ? Fischer Indole Synthesis ? Grignard Reaction ? Henry Nitroaldol Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Jones Oxidation ? Lawesson's Reagent ? Leuckart-Wallach Reaction ? Martin's Sulfurane Dehydrating Reagent ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Mitsunobu Reaction ? Moffatt Oxidation ? Oxidation of Alcohols by DMSO ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Peterson Olefination ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Alcohols ? Preparation of Aldehydes and Ketones ? Preparation of Amines ? Prins Reaction ? Reactions of Alcohols ? Reactions of Aldehydes and Ketones ? Reactions of Amines ? Reactions with Organometallic Reagents ? Reformatsky Reaction ? Ritter Reaction ? Robinson Annulation ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Sharpless Olefin Synthesis ? Specialized Acylation Reagents-Carbodiimides and Related Reagents ? Specialized Acylation Reagents-Ketenes ? Stobbe Condensation ? Swern Oxidation ? Tebbe Olefination ? Ugi Reaction ? Wittig Reaction ? Wolff-Kishner Reduction
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