Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 261762-39-4 | MDL No. : | MFCD01631443 |
Formula : | C7H3ClF2O | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | KPYBGKSDBNMHTO-UHFFFAOYSA-N |
M.W : | 176.55 | Pubchem ID : | 2773509 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
0.42 g | With [bis(acetoxy)iodo]benzene; ammonium acetate; sodium dodecyl-sulfate; In water; at 70℃; for 0.5h; | Example 153A 2-Chloro-3,6-difluorobenzonitrile A mixture of 2-chloro-3,6-difluorobenzaldehyde (1.51 g, 8.5 mmol), sodium lauryl sulfate (0.49 g, 1.71 mmol), (Diacetoxyiodo)benzene (4.12 g, 12.8 mmol) and ammonium acetate (3.29 g, 42.7 mmol) in water (9 mL) was stirred at 70 C. for 30 min After extraction with dichloromethane, the organic phase was dried over magnesium sulfate and concentrated in vacuo. Purification via preparative HPLC (Method 1A) afforded the title compound (0.42 g, 28% of theory) in a purity of 60%. GC-MS (Method 1G): Rt=2.80 min, MS (ESIPos): m/z=175 [M+H]+ |
With [bis(acetoxy)iodo]benzene; ammonium acetate; sodium dodecyl-sulfate; In water; at 70℃; for 0.5h; | A mixture of 2-chloro-3,6-difluorobenzaldehyde (1.51 g, 8.5 mmol), sodium lauryl sulfate (0.49 g, 1.71 mmol), (Diacetoxyiodo)benzene (4.12 g, 12.8 mmol) and ammonium acetate (3.29 g, 42.7 mmol) in water (9 mL) was stirred at 70 C for 30 min. After extraction with dichloromethane, the organic phase was dried over magnesium sulfate and concentrated in vacuo. Purification via preparative HPLC (Method 1A) afforded the title compound (0.42 g, 28% of theory) in a purity of 60%. GC-MS (Method 1G): Rt = 2.80 min, MS (ESIPos): m/z = 175 [M+H]+ |
[ 86522-91-0 ]
2,4-Dichloro-5-fluorobenzaldehyde
Similarity: 0.91
[ 1261869-07-1 ]
2-Chloro-3,4-difluorobenzaldehyde
Similarity: 0.89
[ 86522-91-0 ]
2,4-Dichloro-5-fluorobenzaldehyde
Similarity: 0.91
[ 1261869-07-1 ]
2-Chloro-3,4-difluorobenzaldehyde
Similarity: 0.89
[ 86522-91-0 ]
2,4-Dichloro-5-fluorobenzaldehyde
Similarity: 0.91
[ 1261869-07-1 ]
2-Chloro-3,4-difluorobenzaldehyde
Similarity: 0.89
[ 86522-91-0 ]
2,4-Dichloro-5-fluorobenzaldehyde
Similarity: 0.91
[ 1261869-07-1 ]
2-Chloro-3,4-difluorobenzaldehyde
Similarity: 0.89