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[ CAS No. 2480-23-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 2480-23-1
Chemical Structure| 2480-23-1
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Quality Control of [ 2480-23-1 ]

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Product Details of [ 2480-23-1 ]

CAS No. :2480-23-1 MDL No. :MFCD00037754
Formula : C6H13NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :AKCRVYNORCOYQT-YFKPBYRVSA-N
M.W : 131.17 Pubchem ID :444080
Synonyms :
Chemical Name :N-Methyl-L-valine

Safety of [ 2480-23-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P305+P351+P338 UN#:N/A
Hazard Statements:H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 2480-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2480-23-1 ]

[ 2480-23-1 ] Synthesis Path-Downstream   1~16

  • 2
  • [ 2480-23-1 ]
  • [ 53358-08-0 ]
  • 3
  • [ 42492-62-6 ]
  • [ 2480-23-1 ]
  • 7
  • (2S,2'S)-N-<2'-(methylamino)-3'-methylbutanoyl>bornane-10,2-sultam [ No CAS ]
  • [ 2480-23-1 ]
  • 8
  • [ 2480-23-1 ]
  • [ 79-04-9 ]
  • [ 56346-69-1 ]
  • 9
  • Cyclosporin L [ No CAS ]
  • [ 72-18-4 ]
  • [ 2480-23-1 ]
  • [ 3060-46-6 ]
  • (2s)-2-Amino-2-<(2R,3R)-5-ethyl-2,3,4,5-tetrahydro-3-methylfuryl>essigsaeure [ No CAS ]
  • 10
  • Cyclosporin Z [ No CAS ]
  • [ 72-18-4 ]
  • [ 2480-23-1 ]
  • [ 3060-46-6 ]
  • N-Methyl-L-2-aminooctansaeure [ No CAS ]
  • 11
  • [ 96-81-1 ]
  • [ 74-88-4 ]
  • [ 2480-23-1 ]
  • 12
  • [ 2480-23-1 ]
  • [ 41840-28-2 ]
  • [ 45170-31-8 ]
  • 13
  • [ 2480-23-1 ]
  • [ 41840-29-3 ]
  • Z(OMe)-MeVal-OH [ No CAS ]
  • 14
  • [ 45170-31-8 ]
  • [ 2480-23-1 ]
  • 15
  • [ 2480-23-1 ]
  • [ 79-22-1 ]
  • (2S)-2-[methoxycarbonyl(methyl)amino]-3-methyl-butanoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
71% (2S)-3-Methyl-2-methylamino-butanoic acid (5 g, 38.12 mmol) is added to a stirring solution of sodium hydroxide (76.2 mL of 1 M, 76.24 mmol). After complete dissolution, sodium carbonate (2.1 g, 19.82 mmol) is added followed by methyl chloroformate (3.18 mL, 41.17 mmol) at 0C over 40 minutes. The reaction mixture is stirred at rt for 4 hours, and then washed with diethyl ether (2x 75 ml). The aqueous layer is cooled to 0C, acidified to pH 1 -2 and extracted with CH2Cl2. The organic phase is dried over MgS04, filtered and concentrated to dryness to give the title compound (2S)-2- [methoxycarbonyl(methyl)amino]-3-methyl-butanoic acid (5.12g, 71%) as a clear oil.
  • 16
  • [ 66866-64-6 ]
  • [ 2480-23-1 ]
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