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CAS No. : | 2273-93-0 | MDL No. : | MFCD00039690 |
Formula : | C6H4Cl2N4 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | HVMUWHZAZGTMJK-UHFFFAOYSA-N |
M.W : | 203.03 | Pubchem ID : | 75281 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
58% | With triethylamine; In 1,4-dioxane; at 75℃;Inert atmosphere; | Example 19.2-Chloro-7-methyl-N-(thiazol-2-ylmethyl)-7H-purin-6-amine A mixture of 2,6-dichloro-7-methyl-7H-purine (60 mg, 0.30 mmol), thiazol-2- ylmethanamine dihydrochloride (67 mg, 0.36 mmol) and triethylamine (0.15 mL, 1.05 mmol) in 1,4-dioxane (2 mL) was stirred at 75 C overnight. After this time the mixture was concentrated and the residue purified by column chromatography (silica gel, 0-6% MeOH in CH2Cl2) to afford the title compound as a white solid (48 mg, 58%): ESI MS (M+H) m/z 281; 1H NMR (300 MHz, DMSO-d6) G 8.27 (br s, 2H), 7.75 (d, J = 3.3 Hz, 1H), 7.63 (d, J = 3.3 Hz, 1H), 4.95 (d, J = 5.7 Hz, 2H), 4.03 (s, 3H). |
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