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[ CAS No. 22115-41-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}

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2D 3D

Chemical Structure| 22115-41-9

Chemical Structure| 22115-41-9

Structure of 22115-41-9 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 22115-41-9 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 22115-41-9 ]

SDS Specification

Alternatived Products of [ 22115-41-9 ]

Product Citations

Product Details of [ 22115-41-9 ]

CAS No. :	22115-41-9	MDL No. :	MFCD00001794
Formula :	C₈H₆BrN	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	QGXNHCXKWFNKCG-UHFFFAOYSA-N
M.W :	196.04	Pubchem ID :	89599
Synonyms :		Chemical Name :	2-Cyanobenzyl bromide

Safety of [ 22115-41-9 ]

Signal Word:	Danger	Class:	8
Precautionary Statements:	P301+P330+P331-P303+P361+P353-P363-P304+P340-P310-P321-P260-P264-P280-P305+P351+P338-P405-P501	UN#:	3261
Hazard Statements:	H314	Packing Group:	Ⅱ
GHS Pictogram:

Application In Synthesis of [ 22115-41-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 22115-41-9 ]

[ 22115-41-9 ] Synthesis Path-Downstream 1~3

1
[ 2346-00-1 ]
[ 22115-41-9 ]
2-(4,5-dihydro-1,3-thiazol-2-yl)-1H-3-indenamino [ No CAS ]

Reference： [1]European Journal of Organic Chemistry,2001,p. 1195 - 1201

2
[ 6086-21-1 ]
[ 22115-41-9 ]
[ 1353721-43-3 ]

Reference： [1]Chemistry of Heterocyclic Compounds,2011,vol. 47,p. 996 - 1005

3
[ 22115-41-9 ]
[ 56293-29-9 ]
12-N-(2-cyanobenzyl)aloperine hydrochloride [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
85%		General procedure: Take <strong>[56293-29-9]aloperine</strong> (1) 0.5 g (0,002 mol),Was added to 20 ml of acetonitrile, and 1.8 g (0.006 mol) of anhydrous potassium carbonate and substituted bromobenzyl or benzyl chloride (0.003 mol) were successively added to the reaction solution, followed by stirring at room temperature.TLC was detected until the reaction was complete. The organic phase was concentrated and evaporated to dryness. The solvent was dissolved in dichloromethane and washed successively with water and saturated brine. The methylene chloride layer was dried and the solvent was evaporated to dryness with a rotary evaporator to give the crude 12-N-benzyl <strong>[56293-29-9]aloperine</strong> derivative. The solution was dissolved in 20 ml of methylene chloride solventAnd then separated by column chromatography to give pure product of 12-N-benzyl-<strong>[56293-29-9]aloperine</strong> derivative (2). The resulting compound was dissolved in 5 ml of ether,And then with 1N HCl / Et2O adjusted PH = 6-7, filtered, 12-N-benzyl ether alkalis derivatives pure hydrochloric acid.

Reference： [1]Patent: CN106892920,2017,A .Location in patent: Paragraph 0114; 0115; 0116; 0120; 0121; 0122

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Isomers

Technical Information

? Alkyl Halide Occurrence ? Benzylic Oxidation ? Birch Reduction ? Blaise Reaction ? Blanc Chloromethylation ? Catalytic Hydrogenation ? Complex Metal Hydride Reductions ? Friedel-Crafts Reaction ? General Reactivity ? Grignard Reaction ? Hiyama Cross-Coupling Reaction ? Hydride Reductions ? Hydrogenolysis of Benzyl Ether ? Kinetics of Alkyl Halides ? Kumada Cross-Coupling Reaction ? Preparation of Aldehydes and Ketones ? Preparation of Alkylbenzene ? Preparation of Amines ? Reactions of Alkyl Halides with Reducing Metals ? Reactions of Amines ? Reactions of Benzene and Substituted Benzenes ? Reactions of Dihalides ? Ritter Reaction ? Stille Coupling ? Substitution and Elimination Reactions of Alkyl Halides ? Suzuki Coupling ? Thorpe-Ziegler Reaction ? Vilsmeier-Haack Reaction

Historical Records

Related Functional Groups of
[ 22115-41-9 ]

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Code	Phrase
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P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
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P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
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P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
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P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
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P308 + P313	IF exposed or concerned: Get medical advice/attention.
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P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
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P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
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Storage
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P401
P402	Store in a dry place.
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P402 + P404	Store in a dry place. Store in a closed container.
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P501	Dispose of contents/container to ...
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Ghs Hazard Statements

Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
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H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
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H242	Heating may cause a fire
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H316	Causes mild skin irritation
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H361d	Suspected of damaging the unborn child
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H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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