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CAS No. : | 21187-98-4 | MDL No. : | MFCD00409893 |
Formula : | C15H21N3O3S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | BOVGTQGAOIONJV-UHFFFAOYSA-N |
M.W : | 323.41 | Pubchem ID : | 3475 |
Synonyms : |
S1702;SE1702;S-852;Diaikron;Nordialex;Glimicron;Diamicron
|
Chemical Name : | 1-(Hexahydrocyclopenta[c]pyrrol-2(1H)-yl)-3-[(4-methylphenyl)sulfonyl]urea |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P270-P301+P312+P330-P501 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | In toluene; for 3.0h;Reflux; | To a 250 mL three-necked flask was added N-amino-3-azabicyclo [3.3.0] octane hydrochloride prepared in Example 6 (2)20 g of <strong>[1694-06-0]p-toluenesulfonylurea</strong>, 100 ml of toluene and heated under reflux for 3 hours. After the completion of the reaction,The toluene was distilled off under reduced pressure, 100 ml of water was added, and the crystals were stirred at room temperature for 12 hours. The solid was filtered,Recrystallization from ethyl acetate and drying under vacuum at 80 ° C for 15 h gave 37 g of product, yield 86percent. |