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CAS No. : | 1993-63-1 | MDL No. : | MFCD09264289 |
Formula : | C5H6FN3O | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | BYALTIIVASWNSY-UHFFFAOYSA-N |
M.W : | 143.12 | Pubchem ID : | 44630535 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
95% | With ammonia; In isopropyl alcohol; at 40 - 60℃; | The 32.5g formula III compound are added 170g10wt percent of the isopropyl alcohol solution of ammonia, heating to 40-60°C, stirring reaction 3-5 hours, natural cooling to room temperature, filtered, collecting solid, washing with isopropyl alcohol, drying, the compound of formula II is obtained (kind of white solid) 27.2g, molar yield is 95.0percent, HPLC purity of 99.0percent. |
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