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[ CAS No. 18173-64-3 ] {[proInfo.proName]}

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Chemical Structure| 18173-64-3
Chemical Structure| 18173-64-3
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Szafoni, Ewelina ; Kucinski, Krzysztof ; Hreczycho, Grzegorz DOI:

Abstract: Disclosed is a mild, scalable, and chemoselective cross-dehydrogenative functionalization protocol for the construction of Si?O?Si moieties under cobalt catalysis. The reaction has a broad scope and can be used to synthesize a wide range of silicon building blocks, including challenging dihydrosiloxanes and functionalized silsesquioxanes. Most importantly, the results are placed into context by benchmarking with state-of-the-art methods. Remarkably, the utilized PNP-Co catalyst enables the development of further synthetic strategies such as a one-pot sequential silanolysis/alcoholysis process or unprecedented dehydrocoupling reaction between germanol and hydrosilane.

Keywords: CobaltSilsesquioxanesSiloxanesSilanolsHydrosilanesDehydrogenative coupling

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Stachowiak-Dluzynska, Hanna ; Kucinski, Krzysztof ; Broniarz, Konstancja , et al. DOI: PubMed ID:

Abstract: The reactions between silanols or terminal acetylenes with alkynylgermanes have been accomplished using potassium bis(trimethylsilyl)amide as the catalyst. This strategy has provided an entry point into various organogermanes including germasiloxanes and alkynylgermanes. Remarkably, not only KHMDS but also simple bases such as KOH can serve as efficient catalysts in this process.

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Product Details of [ 18173-64-3 ]

CAS No. :18173-64-3 MDL No. :MFCD00010673
Formula : C6H16OSi Boiling Point : -
Linear Structure Formula :- InChI Key :FGWRMMTYIZKYMA-UHFFFAOYSA-N
M.W : 132.28 Pubchem ID :554527
Synonyms :

Safety of [ 18173-64-3 ]

Signal Word:Danger Class:3
Precautionary Statements:P210-P233-P240-P241-P242-P243-P260-P261-P264-P271-P280-P302+P352-P303+P361+P353-P304-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P340-P362-P370+P378-P403-P403+P233-P403+P235-P405-P501 UN#:1987
Hazard Statements:H225-H315-H319-H335 Packing Group:
GHS Pictogram:
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