成人免费xx,国产又黄又湿又刺激不卡网站,成人性视频app菠萝网站,色天天天天

Home Cart 0 Sign in  

[ CAS No. 1711-07-5 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 1711-07-5
Chemical Structure| 1711-07-5
Structure of 1711-07-5 * Storage: {[proInfo.prStorage]}

Please Login or Create an Account to: See VIP prices and availability

Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Search after Editing

* Storage: {[proInfo.prStorage]}

* Shipping: {[proInfo.prShipping]}

Quality Control of [ 1711-07-5 ]

Related Doc. of [ 1711-07-5 ]

Alternatived Products of [ 1711-07-5 ]
Product Citations

Product Details of [ 1711-07-5 ]

CAS No. :1711-07-5 MDL No. :MFCD00000670
Formula : C7H4ClFO Boiling Point : -
Linear Structure Formula :- InChI Key :SYVNVEGIRVXRQH-UHFFFAOYSA-N
M.W : 158.56 Pubchem ID :74376
Synonyms :

Safety of [ 1711-07-5 ]

Signal Word:Danger Class:8
Precautionary Statements:P260-P264-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P321-P363-P405-P501 UN#:3265
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 1711-07-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 1711-07-5 ]
  • Downstream synthetic route of [ 1711-07-5 ]

[ 1711-07-5 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 6638-79-5 ]
  • [ 1711-07-5 ]
  • [ 226260-01-1 ]
YieldReaction ConditionsOperation in experiment
86.5% With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere To a solution of Ν,Ο-dimethylhydroxylamine hydrochloride (138 g, 1.42 mol) in DCM (1.5 L) was added Et3N (383 g, 3.78 mol) at room temperature (RT). To the stirred mixture, 1-1 (150 g, 946 mmol) was added dropwise at 0 °C under N2 atmosphere. The solution was stirred at the same temperature for 1 h, and then slowly warmed to RT for 10 h. The mixture was added to water (~1L) and extracted with EtOAc (2 x 500 mL). The combined organic phases were dried with Na2S04, filtered and concentrated. The residue was purified by flash column chromatography (eluent: PE) to give 1-2 as a white solid (150 g, yield: 86.5percent). 1H NMR (400 MHz, CDC13): δ 7.49-7.43 (1 H, m), 7.41-7.32 (2 H, m), 7.18- 7.10 (1 H, m), 3.54 (3 H, s), 3.34 (3 H, s).
Reference： [1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 4, p. 1415 - 1419
[2] Patent: WO2016/145103, 2016, A1, . Location in patent: Paragraph 0165
[3] Patent: US6174874, 2001, B1,
[4] Patent: US2008/249095, 2008, A1, . Location in patent: Page/Page column 44
  • 2
  • [ 1711-07-5 ]
  • [ 226260-01-1 ]
YieldReaction ConditionsOperation in experiment
86.5% With triethylamine In dichloromethane at 0 - 20℃; for 11 h; Inert atmosphere 10264] To a solution of N,O-dimethylhydroxylamine hydrochloride (138 g, 1.42 mol) in DCM (1.5 L) was addedEt3N (383 g, 3.78 mol) at RT. To the stirred mixture, G-1 (150 g, 946 mmol) was added dropwise at 00 C. under N2 atmosphere. The solution was stirred at the same temperature for 1h, and then slowly warmed to RT for 10 h. The mixture wasadded to water (.—1 L) and extracted with EtOAc (2x500 mE).The combined organic phases were dried with Na2504, filtered and concentrated. The residue was purified by flashcolunm chromatography (eluent: PE) to give G-2 as a white solid (150 g, yield: 86.5percent). ‘H NMR (400 MHz, CDC13): ? 7.49-7.43 (1H, m), 7.41-7.32 (2H, m), 7.18-7.10 (1H, m),3.54 (3H, s), 3.34 (3H, s).
Reference： [1] Patent: US2015/72982, 2015, A1, . Location in patent: Paragraph 0263; 0264
Recommend Products
Same Skeleton Products

Technical Information

Historical Records
; ;