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[ CAS No. 14425-64-0 ] {[proInfo.proName]}

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Chemical Structure| 14425-64-0
Chemical Structure| 14425-64-0
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Product Details of [ 14425-64-0 ]

CAS No. :14425-64-0 MDL No. :MFCD07369786
Formula : C9H11BrO Boiling Point : No data available
Linear Structure Formula :- InChI Key :OXHPTABOQVHKLN-UHFFFAOYSA-N
M.W : 215.09 Pubchem ID :84427
Synonyms :

Safety of [ 14425-64-0 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P270-P301+P312+P330-P501 UN#:
Hazard Statements:H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 14425-64-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14425-64-0 ]

[ 14425-64-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 14425-64-0 ]
  • [ 124-40-3 ]
  • [ 539-15-1 ]
YieldReaction ConditionsOperation in experiment
40% A solution of 4-methoxyphenethyl bromide (0.20 g, 0.93 mmol) and dimethylamine (2.0 M in THF, 2 ml) was stirred in a sealed-tube at rt for 18 h. The reaction mixture was concentrated in vacuo and re-dissolved in dichloromethane (2 ml). After cooling to 0 C., boron tribromide (1.0 M in hexane, 1.00 ml) was added dropwise, and the solution was stirred at this temperature for 10 min. Water (20 ml) was added dropwise and the mixture was stirred for further 30 min. After warming to rt, the reaction mixture was extracted with dichloromethane (3×20 ml). The combined organic layers were washed with brine (30 ml), dried over sodium sulfate, and then concentrated in vacuo. Purification by flash chromatography on silica (aqueous ammonia solution/methanol/dichloromethane, 5:20:75) afforded the titled compound as a white solid (61 mg, 40%).1H NMR (400 MHz; CD4OD) 2.31 (6H, s), 2.54 (2H, m, CH2), 2.65 (2H, m, CH2), 6.67 (2H, d, J 8.4 Hz, Ph-H), 6.99 (2H, d, J 8.4 Hz, Ph-H);13C NMR (100 MHz; CD4OD) 34.5, 46.1, 63.5, 117.2, 131.4 and 132.3, 157.8;m/z (+ES) 166 (100, MH+).
  • 2
  • [ 6374-91-0 ]
  • [ 14425-64-0 ]
  • [ 1020264-99-6 ]
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