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CAS No. : | 14221-02-4 | MDL No. : | MFCD00010014 |
Formula : | C72H60P4Pt | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | SYKXNRFLNZUGAJ-UHFFFAOYSA-N |
M.W : | 1244.23 | Pubchem ID : | 11979705 |
Synonyms : |
|
Chemical Name : | Tetrakis(triphenylphosphine)platinum(0) |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79% | In toluene; at 20℃;Inert atmosphere; Schlenk technique; | General procedure: [M(PPh3)4] (1.0 equiv.) was added as a solid to a toluene solution (15mL) of 1 or 2 (1.0 equiv.) in a Schlenk flask and was stirred overnight at room temperature. The solvent was removed under the vacuum. The resulted yellow residue was dissolved in DCM (2mL) and was precipitated by addition of n-pentane (15mL), filtered and dried in vacuum to afford the product as yellow powder. |