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[ CAS No. 14096-51-6 ] {[proInfo.proName]}

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Chemical Structure| 14096-51-6
Chemical Structure| 14096-51-6
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Product Details of [ 14096-51-6 ]

CAS No. :14096-51-6 MDL No. :MFCD00000011
Formula : C2H8Cl2N2Pt Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 326.08 Pubchem ID :-
Synonyms :

Safety of [ 14096-51-6 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 14096-51-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14096-51-6 ]

[ 14096-51-6 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 14096-51-6 ]
  • [ 107-15-3 ]
  • [Pt(ethane-1,2-diamine)2]Cl2 [ No CAS ]
  • 2
  • [ 10025-99-7 ]
  • [ 107-15-3 ]
  • [ 14096-51-6 ]
YieldReaction ConditionsOperation in experiment
77% for 1h;Inert atmosphere; To a stirred aqueous solution (10 ml) of K2PtCl4 (0.815 g, 1.96 mmol), ehtyelenediamine(0.5 ml, 0.45 g, 7.49 mmol) was added drop-wise at room temperature and stirred for 1 hwhereupon a pale yellow precipitate formed. The suspension was centrifuged and the yellowprecipitate was separated and washed with distilled water (3 x 10 ml) followed by ethyl alcoholaliquots (2 x 10 ml) and dried in vacuo to give pale yellow compound (0.49 g, 77 %).
55% In water; for 48h;Darkness; General procedure: The solution of L was added dropwise to the water solution of K2PtCl4 at constant stirring. After the addition of the ligand, the solution was stirred for 2 days away from light. The precipitation was filtered, washed several times with ethyl ether and dried in vacuum desiccator.
With hydrogenchloride; In water; at 80℃; for 2h;pH Ca. 3; General procedure: All mononuclear Pt(II) complexes were prepared with minor modification of a method previously used in our laboratory for the preparation of a series of [M(L)Cl2] complexes (M is Pt(II) or Pd(II); L is bidentate coordinated diamine or amino acid) [15,23,33]. K2PtCl4 was dissolved in water and mixed with an equimolar amount of diamine ligand (L). The pH of the solution was adjusted to ca. 3 by addition of 1M HCl and mixture was stirred at 80C for 2h. All complexes were crystallized from water at room temperature. The pure complexes were obtained by recrystallization from warm water and than cooling at room temperature. The experimental results of the elemental analyses for C, H and N parameters for all investigated Pt(II) complexes are in accordance with theoretical values calculated for [Pt(L)Cl2] complexes.
With hydrogenchloride; In water; at 100℃; for 15h; In a 50 mL three-necked flask,Adding 0.2 g of potassium tetrachlorostate and 20 mL of a 50 mM hydrochloric acid solution,Then, 200 μL of ethylenediamine was added, the mixture was magnetically stirred,100 C reflux reaction 15 h; after the reaction is cooled to room temperature, filtration,The resulting solid was washed three times with ethanol and then vacuum dried at 50 C for 12 h,To obtain a yellow dichloro (ethylenediamine) platinum complex;

  • 3
  • [Pt(ethane-1,2-diamine)2]Cl2 [ No CAS ]
  • [ 14096-51-6 ]
  • 5
  • [ 14096-51-6 ]
  • [ 141-82-2 ]
  • [ 41666-77-7 ]
  • 6
  • [ 14096-51-6 ]
  • [Pt(ethane-1,2-diamine)2]Cl2 [ No CAS ]
  • 7
  • [ 14096-51-6 ]
  • [ 763040-08-0 ]
  • 10
  • [ 14096-51-6 ]
  • [ 58-63-9 ]
  • [ 80263-30-5 ]
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