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CAS No. : | 136-85-6 | MDL No. : | MFCD00005702 |
Formula : | C7H7N3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | LRUDIIUSNGCQKF-UHFFFAOYSA-N |
M.W : | 133.15 | Pubchem ID : | 8705 |
Synonyms : |
|
Chemical Name : | 5-Methyl-1H-benzo[d][1,2,3]triazole |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P501-P270-P264-P280-P337+P313-P305+P351+P338-P302+P352-P332+P313-P362-P301+P312+P330 | UN#: | N/A |
Hazard Statements: | H302-H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium hydroxide; In water; at 45 - 65℃; for 10h; | Tolyltriazole (26.63 g. 200 mmol) and 3-chloro-2-hydroxy-l-propanesulfonic acid sodium salt hydrate (43.25 g, 220 mmol) are dissolved in 160 mL of distilled water at room temperature. To the stirred solution is added 16.0 g of 50% aqueous sodium hydroxide solution dropwise, and the solution is heated to 45 C for four hours and then held at 65 C for six hours. The solution is allowed to cool to room temperature and 137 g of distilled water is added. The solution is determined to be 25.45% solids. |
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