[ CAS No. 13515-93-0 ] {[proInfo.proName]}

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2D 3D

Structure of 13515-93-0 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 13515-93-0 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 13515-93-0 ]

SDS Specification

Alternatived Products of [ 13515-93-0 ]

Product Details of [ 13515-93-0 ]

CAS No. :	13515-93-0	MDL No. :	MFCD00038876
Formula :	C₄H₁₀ClNO₂	Boiling Point :	-
Linear Structure Formula :	CH₃NHCH₂CO₂CH₃·HCl	InChI Key :	HQZMRJBVCVYVQA-UHFFFAOYSA-N
M.W :	139.58	Pubchem ID :	83544
Synonyms :		Chemical Name :	Methyl N-methylglycinate hydrochloride

Calculated chemistry of [ 13515-93-0 ] Expand+

Physicochemical Properties

Num. heavy atoms :	8
Num. arom. heavy atoms :	0
Fraction Csp3 :	0.75
Num. rotatable bonds :	3
Num. H-bond acceptors :	3.0
Num. H-bond donors :	1.0
Molar Refractivity :	32.39
TPSA :	38.33 ?2

Pharmacokinetics

GI absorption :	High
BBB permeant :	No
P-gp substrate :	No
CYP1A2 inhibitor :	No
CYP2C19 inhibitor :	No
CYP2C9 inhibitor :	No
CYP2D6 inhibitor :	No
CYP3A4 inhibitor :	No
Log Kp (skin permeation) :	-6.78 cm/s

Lipophilicity

Log Po/w (iLOGP) :	0.0
Log Po/w (XLOGP3) :	0.52
Log Po/w (WLOGP) :	0.18
Log Po/w (MLOGP) :	0.01
Log Po/w (SILICOS-IT) :	-0.35
Consensus Log Po/w :	0.07

Druglikeness

Lipinski :	0.0
Ghose :	None
Veber :	0.0
Egan :	0.0
Muegge :	2.0
Bioavailability Score :	0.55

Water Solubility

Log S (ESOL) :	-0.84
Solubility :	20.4 mg/ml ; 0.146 mol/l
Class :	Very soluble
Log S (Ali) :	-0.9
Solubility :	17.7 mg/ml ; 0.127 mol/l
Class :	Very soluble
Log S (SILICOS-IT) :	-0.73
Solubility :	26.2 mg/ml ; 0.188 mol/l
Class :	Soluble

Medicinal Chemistry

PAINS :	0.0 alert
Brenk :	0.0 alert
Leadlikeness :	1.0
Synthetic accessibility :	1.03

Safety of [ 13515-93-0 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 13515-93-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 13515-93-0 ]
Downstream synthetic route of [ 13515-93-0 ]

[ 13515-93-0 ] Synthesis Path-Upstream 1~2

1
[ 24424-99-5 ]
[ 13515-93-0 ]
[ 42492-57-9 ]

Yield	Reaction Conditions	Operation in experiment
90%	With triethylamine In dichloromethane at 0 - 20℃; for 48 h; Inert atmosphere	To a suspension of sarcosine (35.64 g, 0.40 mol) in 350 mL MeOH was added thionyl chloride (29.02 mL, 0.40 mol) dropwise at 0 °C. After complete addition the cooling bath was removed and the reaction mixture was stirred for 30 min at r.t. and refluxed for further 6 h. The resulting solution was concentrated in vacuum and the residue was dried in high vacuum over night at r.t. to afford sarcosine methyl ester.HCl as a white powder which was used in the next step without further purification; yield: 56.14 g (quant.); mp. 102 °C. 1H-NMR (300 MHz, CDCl3): δ = 9.76 (s, 2 H, NH2), 3.88 (t, J = 5.6 Hz, 2 H, H-2), 3.82 (s, 3 H, H-4)), 2.83 (t, J = 5.2 Hz, 3 H, H-3). 13C-NMR(75 MHz, CDCl3): δ = 166.7 (C-1), 53.3 (C-2), 48.9 (C-3), 33.4 (C-4).1 To a suspension of sarcosine methylester.HCl (59.80 g, 0.43 mol) and (Boc)2O (138.01 mL, 0.65 mol) in 1.0 L CH2Cl2 TEA (119.09 mL, 0.86 mol) was added dropwise at 0 °C. After complete addition the cooling bath was removed and the reaction mixture was stirred for two days at r.t. Aq. HCl (1 M) was added until the aqueous layer showed pH = 6. The resulting two layers were separated and the organic layer was washed with dist. H2O, dried (Na2SO4), concentrated in vacuum and volatile impurities were removed in high vacuum over night at r.t. to afford a clear oil; yield: 78.65 g (90 percent)

Reference： [1] Synthesis (Germany), 2017, vol. 49, # 4, p. 770 - 774
[2] Patent: EP1032561, 2004, B1, . Location in patent: Page 21

2
[ 1070-19-5 ]
[ 13515-93-0 ]
[ 42492-57-9 ]

Reference： [1] Gazzetta Chimica Italiana, 1977, vol. 107, p. 381 - 385

[ 13515-93-0 ] Synthesis Path-Downstream 1~6

1
[ 56612-14-7 ]
[ 13515-93-0 ]
[ 65918-86-7 ]

Reference： [1]Gazzetta Chimica Italiana,1977,vol. 107,p. 381 - 385

2
[ 13515-93-0 ]
[ 141871-02-5 ]
Boc Me Ant-Sar-OMe [ No CAS ]

Reference： [1]Synthetic Communications,1993,vol. 23,p. 2265 - 2272

3
[ 119479-32-2 ]
[ 13515-93-0 ]
[ 889128-01-2 ]

Yield	Reaction Conditions	Operation in experiment
70%	With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20℃; for 3.16667h;	(rαc.)-[(2-terMButoxycarbonylamino-pent-4-enoyl)methylamino]acetic acid methyl ester (B); PyBop (24.06g; 46.3 mmol) was added to a sol. of compound B (9.00 g; 42.04mmol) in DMF (200 mL) nnder N2 at rt. The sol. was stirred for 10 min at rt, and sarcosine methylester hydrochloride (6.46g; 46.3 mmol) and DIPEA (23.8 mL; 139 mmol) were added dropwise. The mixture was stirred at rt for 3 hours. EtOAc (400 mL) was added and the resulting organic phase was washed with brine (3x). The combined org. layers were dried over MgSO4, filtered, and the solvents were removed under reduced pressure. The crude product was diluted again in EtOAc (150 mL) and the mixture was washed with water (2x). The combined org. layers were dried over MgSO4, filtered, and the solvents were removed under reduced pressure. Purification of the residue by FC (CH2Cl2/Me0H 50:1) yielded the title compound (8.82 g, 70%)

Reference： [1]Patent: WO2006/58546,2006,A1 .Location in patent: Page/Page column 13

4
[ 4316-94-3 ]
[ 13515-93-0 ]
methyl N-(6-amino-5-nitropyrimidin-4-yl)-N-methylglycinate [ No CAS ]

Reference： [1]Tetrahedron Letters,2005,vol. 46,p. 1841 - 1844
[2]Journal of Heterocyclic Chemistry,2006,vol. 43,p. 267 - 276

5
[ 6608-47-5 ]
[ 13515-93-0 ]
(ethenesulfonylmethylamino)acetic acid methyl ester [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
20%	With dmap; triethylamine; In dichloromethane; at 0 - 20℃; for 2.16667h;Inert atmosphere;	Triethylamine (1.93 ml; 14.0 mmol) and 4-(Dimethylamino) pyridine (0.085 g; 0.70 mrnol) were added under argon-atmosphere to a cold solution of sarcosinmethylester Hydrochlorid (0.650 g; 4.66 mmol) in 9 ml DCM. Then<strong>[6608-47-5]ethenesulfonyl chloride</strong> (0.456 ml; 5.12 mmol) was added drop wise over 10 mm at 0C - 5C (exotherm reaction) under stirring. The yellow reaction-suspension was stirred at 0C for 1 h and then for 1 h at RT before water was added under ice- cooling. The organic phase was washed with water (2x) and brine (lx), dried over Na2SO4, filtrated and evaporated. Purification by flash chromatography (25gSilica-Gel heptane/ 0-100% ethyl acetate in 25 mm) gave 183 mg (20%) of thetitle compound as colourless oil.HPLC (Chromolith Performance RP-18e 100-4.6 HPLC-elite; 5mm 4m1 215nm;4ml/min, 215nm, buffer A 0.05% TFAIH2O, buffer B 0.04% TFAIACN, 0.0-0.2 mm5% buffer B; 0.2-5.0 mm 5%-100% buffer B; 5.0-5.5 mm 99%-5% buffer B):(percent area) 99.6 %; Rt 1.89 mm.LC/MS (Chromolith Speed Rod RP 18e 50-4.6 mm; Polar.m, 2.4m1/min, 220nm, buffer A 0.05% HCOOH/H20, buffer B 0.04% HCOOH/ACN, 0.0-2.8mm 4%- 100% buffer B; 2.8-3.3mm 100% buffer B 3.3-3.4mm 100%-4% buffer B): Rt 1.31 mm; (M+H) 194.1.

Reference： [1]Patent: WO2016/50358,2016,A1 .Location in patent: Page/Page column 102; 103

6
[ 19064-24-5 ]
[ 13515-93-0 ]
2-[(3-fluoro-2-nitrophenyl)(methyl)amino]acetic acid [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
88%	With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 50℃;	To a solution of l,3-difluoro-2-nitrobenzene (5 g, 31.428 mmol, 1 equiv) in dimethylsulfoxide (50 mL) was added methyl 2-(methylamino)acetate hydrochloride (4.83 g, 34.571 mmol, 1.1 equiv) and DIEA (12.19 g, 94.285 mmol, 3 equiv). The resulting mixture was stirred at 50oC overnight. The mixture was cooled to RT and diluted with water. The pH value of the solution was adjusted to 3 with HC1 (1 M) and extracted with ethyl acetate. The combined organic layers were washed with brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. This resulted in 6.3 g (88%) of 56.1 as a yellow solid. (ES, m/z): 227 (M-H).

Reference： [1]Patent: WO2020/132566,2020,A1 .Location in patent: Paragraph 00457-00458

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Precautionary Statements-General
Code	Phrase
P101	If medical advice is needed,have product container or label at hand.
P102	Keep out of reach of children.
P103	Read label before use
Prevention
Code	Phrase
P201	Obtain special instructions before use.
P202	Do not handle until all safety precautions have been read and understood.
P210	Keep away from heat/sparks/open flames/hot surfaces. - No smoking.
P211	Do not spray on an open flame or other ignition source.
P220	Keep/Store away from clothing/combustible materials.
P221	Take any precaution to avoid mixing with combustibles
P222	Do not allow contact with air.
P223	Keep away from any possible contact with water, because of violent reaction and possible flash fire.
P230	Keep wetted
P231	Handle under inert gas.
P232	Protect from moisture.
P233	Keep container tightly closed.
P234	Keep only in original container.
P235	Keep cool
P240	Ground/bond container and receiving equipment.
P241	Use explosion-proof electrical/ventilating/lighting/equipment.
P242	Use only non-sparking tools.
P243	Take precautionary measures against static discharge.
P244	Keep reduction valves free from grease and oil.
P250	Do not subject to grinding/shock/friction.
P251	Pressurized container: Do not pierce or burn, even after use.
P260	Do not breathe dust/fume/gas/mist/vapours/spray.
P261	Avoid breathing dust/fume/gas/mist/vapours/spray.
P262	Do not get in eyes, on skin, or on clothing.
P263	Avoid contact during pregnancy/while nursing.
P264	Wash hands thoroughly after handling.
P265	Wash skin thouroughly after handling.
P270	Do not eat, drink or smoke when using this product.
P271	Use only outdoors or in a well-ventilated area.
P272	Contaminated work clothing should not be allowed out of the workplace.
P273	Avoid release to the environment.
P280	Wear protective gloves/protective clothing/eye protection/face protection.
P281	Use personal protective equipment as required.
P282	Wear cold insulating gloves/face shield/eye protection.
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P284	Wear respiratory protection.
P285	In case of inadequate ventilation wear respiratory protection.
P231 + P232	Handle under inert gas. Protect from moisture.
P235 + P410	Keep cool. Protect from sunlight.
Response
Code	Phrase
P301	IF SWALLOWED:
P304	IF INHALED:
P305	IF IN EYES:
P306	IF ON CLOTHING:
P307	IF exposed:
P308	IF exposed or concerned:
P309	IF exposed or if you feel unwell:
P310	Immediately call a POISON CENTER or doctor/physician.
P311	Call a POISON CENTER or doctor/physician.
P312	Call a POISON CENTER or doctor/physician if you feel unwell.
P313	Get medical advice/attention.
P314	Get medical advice/attention if you feel unwell.
P315	Get immediate medical advice/attention.
P320
P302 + P352	IF ON SKIN: wash with plenty of soap and water.
P321
P322
P330	Rinse mouth.
P331	Do NOT induce vomiting.
P332	IF SKIN irritation occurs:
P333	If skin irritation or rash occurs:
P334	Immerse in cool water/wrap n wet bandages.
P335	Brush off loose particles from skin.
P336	Thaw frosted parts with lukewarm water. Do not rub affected area.
P337	If eye irritation persists:
P338	Remove contact lenses, if present and easy to do. Continue rinsing.
P340	Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P341	If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
P360	Rinse immediately contaminated clothing and skin with plenty of water before removing clothes.
P361	Remove/Take off immediately all contaminated clothing.
P362	Take off contaminated clothing and wash before reuse.
P363	Wash contaminated clothing before reuse.
P370	In case of fire:
P371	In case of major fire and large quantities:
P372	Explosion risk in case of fire.
P373	DO NOT fight fire when fire reaches explosives.
P374	Fight fire with normal precautions from a reasonable distance.
P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
P377	Leaking gas fire: Do not extinguish, unless leak can be stopped safely.
P378
P380	Evacuate area.
P381	Eliminate all ignition sources if safe to do so.
P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P401
P402	Store in a dry place.
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P413
P420	Store away from other materials.
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P402 + P404	Store in a dry place. Store in a closed container.
P403 + P233	Store in a well-ventilated place. Keep container tightly closed.
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P410 + P412	Protect from sunlight. Do not expose to temperatures exceeding 50 oC/122oF.
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Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
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H222	Extremely flammable aerosol
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H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
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H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
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H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
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H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
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H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
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H320	Causes eye irritation
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H361d	Suspected of damaging the unborn child
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H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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[ CAS No. 13515-93-0 ] {[proInfo.proName]}

Quality Control of [ 13515-93-0 ]

Related Doc. of [ 13515-93-0 ]

Product Details of [ 13515-93-0 ]

Calculated chemistry of [ 13515-93-0 ] Expand+

Physicochemical Properties

Pharmacokinetics

Lipophilicity

Druglikeness

Water Solubility

Medicinal Chemistry

Safety of [ 13515-93-0 ]

Application In Synthesis of [ 13515-93-0 ]

[ 13515-93-0 ] Synthesis Path-Upstream 1~2

[ 13515-93-0 ] Synthesis Path-Downstream 1~6

Similar Product of [ 13515-93-0 ]

Related Functional Groups of [ 13515-93-0 ]

Amino Acid Derivatives

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Similar Product of
[ 13515-93-0 ]

Related Functional Groups of
[ 13515-93-0 ]