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CAS No. : | 13316-12-6 | MDL No. : | MFCD16657018 |
Formula : | C5H2ClN3S | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | HGYFXAHDBRHZGF-UHFFFAOYSA-N |
M.W : | 171.61 | Pubchem ID : | 263007 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
27% | With hydrogenchloride; In 1,4-dioxane; isopropyl alcohol; at 100℃; for 0.5h;Microwave irradiation; | 7-Chlorothiazolo[5,4-d]pyrimidine (50 mg, 0.29 mmol), <strong>[2343-22-8]5-fluoroindoline</strong> (42 mg, 0.31 mmol), 4M HCI in dioxane (0.075 ml) in IPA (0.7ml) were irradiated in the microwave at 100 C for 30 mm. The precipitate was filtered and washed with methanol. The residuewas purified by filtration through an aminopropyl cartridge eluting with DCM:MeOH (10:1) to give a green solid (23 mg, 27%). 1H NMR (400 MHz, DM50-cl6) 6 ppm 3.29 (t, J=8.47 Hz, 2 H), 4.74 - 4.92 (m, 2 H), 7.08 (td, J9.16, 2.75 Hz, I H), 7.15 - 7.26 (m, I H), 8.61 (dd, J8.93, 4.81 Hz, I H), 8.64 (s, I H), 9.34 (s, I H). |
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