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[ CAS No. 1309666-78-1 ] {[proInfo.proName]}

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Chemical Structure| 1309666-78-1
Chemical Structure| 1309666-78-1
Structure of 1309666-78-1 * Storage: {[proInfo.prStorage]}

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Product Details of [ 1309666-78-1 ]

CAS No. :1309666-78-1 MDL No. :MFCD22201525
Formula : C16H24O6S Boiling Point : -
Linear Structure Formula :- InChI Key :OVLSSENVXOKYAD-UHFFFAOYSA-N
M.W : 344.42 Pubchem ID :60146215
Synonyms :
Chemical Name :tert-Butyl 3-(2-(tosyloxy)ethoxy)propanoate

Safety of [ 1309666-78-1 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1309666-78-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1309666-78-1 ]

[ 1309666-78-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 104-15-4 ]
  • [ 671802-00-9 ]
  • [ 1309666-78-1 ]
  • 2
  • [ 98-59-9 ]
  • [ 671802-00-9 ]
  • [ 1309666-78-1 ]
YieldReaction ConditionsOperation in experiment
55% With triethylamine; In tetrahydrofuran; at 0 - 20℃; for 16h; To a solution of Compound (g-2) (0.20 g, 1.1 mmol) and triethylamine (0.31 g, 3.2 mmol) in THF (15 mL) was added p-toluenesulfonyl chloride (0.30 g, 1.6 mmol) at 0 C. over 10 minutes, and then the reaction mixture was stirred at at room temperature 16 hours. The solvent was removed in vacuo, and the residue was purified by preparative TLC (pentane:ethyl acetate=4:1) to give Compound (h-1) (0.20 g, 55% yield). (1098) 1H-NMR (CDCl3, 400 MHz) delta: 7.71 (d, J=8.2 Hz, 2H), 7.27 (d, J=8.2 Hz, 2H), 4.07-4.05 (m, 2H), 3.55-3.54 (m, 4H), 2.39-2.33 (m, 5H), 1.36 (s, 9H).
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