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CAS No. : | 118427-29-5 | MDL No. : | MFCD00013461 |
Formula : | C9H15ClN2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | LMFPPUVGWDZXMB-UHFFFAOYSA-N |
M.W : | 186.68 | Pubchem ID : | 2733248 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302+H312+H332-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
35% | In methanol; at 20℃; | General procedure: Suitable indoline-2,3-dione 1a-c (1.0 mmol) was dissolved in methanol (5 mL) with gentle heating, then arylhydrazine (2.4 mmol) was slowly added with stirring at room temperature. After stirring overnight, the resulting precipitate was filtered and crystallized or the reaction mixture was evaporated to dryness and the residue suitably purified. |
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