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ChemicalBook >> CAS DataBase List >>5-Fluoro-2-methylaniline

5-Fluoro-2-methylaniline

CAS No.
367-29-3
Chemical Name:
5-Fluoro-2-methylaniline
Synonyms
2-AMINO-4-FLUOROTOLUENE;2-METHYL-5-FLUOROANILINE;2-Amino-4-fluorotoluene~5-Fluoro-o-toluidine;TIMTEC-BB SBB004266;5-Fluoro-2-toluidine;5-Fluoro-2-methylani;Fluoromethylaniline7;5-FLUORO-O-TOLUIDINE;4-Fluoro-2-Aminotoluene;5-FLUORO-2-METHYLANILINE
CBNumber:
CB8263018
Molecular Formula:
C7H8FN
Molecular Weight:
125.14
MDL Number:
MFCD00007764
MOL File:
367-29-3.mol
MSDS File:
SDS
Last updated:2024-06-18 21:58:05

5-Fluoro-2-methylaniline Properties

Melting point 38-40 °C (lit.)
Boiling point 98-100°C 15mm
Density 1.13 g/cm3 (20℃)
refractive index 1.538
Flash point 194 °F
storage temp. Keep in dark place,Inert atmosphere,2-8°C
form Crystalline Solid or Liquid
pka 3.44±0.10(Predicted)
color Purple to brown
Water Solubility insoluble
BRN 2637584
InChI InChI=1S/C7H8FN/c1-5-2-3-6(8)4-7(5)9/h2-4H,9H2,1H3
InChIKey JLCDTNNLXUMYFQ-UHFFFAOYSA-N
SMILES C1(N)=CC(F)=CC=C1C
CAS DataBase Reference 367-29-3(CAS DataBase Reference)
NIST Chemistry Reference 5-Fluoro-2-methylaniline(367-29-3)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictogramsGHS hazard pictogramsGHS hazard pictograms
GHS07,GHS06,GHS08
Signal word  Warning
Hazard statements  H302+H312+H332-H315-H319-H335-H302-H311-H332-H373
Precautionary statements  P261-P280-P301+P312+P330-P305+P351+P338-P260-P304+P340-P405-P501a-P264-P270-P271-P302+P352+P312+P362+P364-P304+P340+P312-P305+P351+P338+P337+P313-P501
Hazard Codes  Xn,T,Xi
Risk Statements  20/21/22-36/37/38-23/24/25
Safety Statements  26-27-36/37/39-45-36
RIDADR  UN 1325 4.1/PG 2
WGK Germany  3
Hazard Note  Toxic/Irritant
HazardClass  6.1
PackingGroup  III
HS Code  29214300
NFPA 704
2
3 0

5-Fluoro-2-methylaniline price More Price(29)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich F10402 5-Fluoro-2-methylaniline 99% 367-29-3 10g $31.8 2023-01-07 Buy
TCI Chemical F0232 5-Fluoro-2-methylaniline >98.0%(GC) 367-29-3 5g $27 2024-03-01 Buy
TCI Chemical F0232 5-Fluoro-2-methylaniline >98.0%(GC) 367-29-3 25g $78 2024-03-01 Buy
Alfa Aesar B25381 5-Fluoro-2-methylaniline, 98% 367-29-3 10g $42.65 2024-03-01 Buy
Alfa Aesar B25381 5-Fluoro-2-methylaniline, 98% 367-29-3 50g $141.65 2024-03-01 Buy
Product number Packaging Price Buy
F10402 10g $31.8 Buy
F0232 5g $27 Buy
F0232 25g $78 Buy
B25381 10g $42.65 Buy
B25381 50g $141.65 Buy

5-Fluoro-2-methylaniline Chemical Properties,Uses,Production

Chemical Properties

purple to brown crystalline solid

Uses

Used as a pharmaceutical intermediate in organic synthesis.

Synthesis

In a nitrogen-fed glovebox, Pd(P(o-tol)3)2 and CyPF-PtBu (1:1 ratio) were dissolved in dioxane and mixed for 5 min. A 20 mL scintation vial was charged with aryl halide (0.60 mmol, 1 equiv), ammonium sulfate (0.90 mmol, 1.5 equiv), and sodium tert-butoxide (2.7 mmol, 4.5 equiv). To this vial was added 6 mL of anhydrous dioxane and the appropriate amount of catalyst from the stock solution. The reaction vial was sealed with a Teflon-lined screw cap and removed from the glovebox. The reaction was stirred at the desired temperature for 12 h. The reaction mixture was diluted with EtOAc and filtered through a pad of Celite. The filtrate was concentrated in vacuo, and the crude product was purified by flash column chromatography. 5-Fluoro-2-methylaniline (Table 3, 2s) (CAS: 367-29-3) The reaction to form this product was conducted with 0.5 mol % Pd(P(o-tol)3)2 and 0.5 mol % CyPF-PtBu for 8 h. The crude product was isolated by flash column chromatography (5:1 Hexanes:EtOAc). 5-Fluoro-2-methylaniline was isolated as an oil in 76% yield. 1(600 MHz, CDCl3): δ 6.97 (t, J= 7.2 Hz, 1H), 6.40 (t, J= 9.9 Hz, 2H), 3.69 (s, 2H), 2.12 (s, 3H). 13C-NMR(151 MHz, CDCl3): δ 162.24 (d, JC-F= 240.9 Hz), 145.82 (d, JC-F= 10.6 Hz), 131.12 (d, JC-F= 9.6 Hz), 117.62 (d, JC-F = 2.6 Hz), 104.67 (d, JC-F= 21.0 Hz), 101.56 (d, JC-F= 24.6 Hz), 16.62 (s).
5-Fluoro-2-methylaniline synthesis

446-10-6
367-29-3
Synthesis of 5-Fluoro-2-methylaniline from 4-Fluoro-2-nitrotoluene
Global( 339)Suppliers
Supplier Tel Email Country ProdList Advantage
Shaanxi Dideu Medichem Co. Ltd
+86-029-81138252 +86-18789408387 1057@dideu.com China 3958 58
Hi-Tech Chemistry Corp
0519-86626038 yuhh@hitechem.com CHINA 810 58
Nanjing ChemLin Chemical Industry Co., Ltd.
025-83697070 product@chemlin.com.cn CHINA 3009 60
ATK CHEMICAL COMPANY LIMITED
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career henan chemical co
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Chongqing Chemdad Co., Ltd
+86-023-6139-8061 +86-86-13650506873 sales@chemdad.com China 39894 58
Alchem Pharmtech,Inc.
8485655694 sales@alchempharmtech.com United States 63687 58
CONIER CHEM AND PHARMA LIMITED
+8618523575427 sales@conier.com China 49374 58
Richest Group Ltd
18017061086 oled@richest-group.com CHINA 5600 58

View Lastest Price from 5-Fluoro-2-methylaniline manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
5-Fluoro-2-methylaniline pictures 2024-06-18 5-Fluoro-2-methylaniline
367-29-3
US $1.00 / KG 1KG 99% 20t Shaanxi Dideu Medichem Co. Ltd
5-Fluoro-2-methylaniline pictures 2022-09-28 5-Fluoro-2-methylaniline
367-29-3
US $0.00-0.00 / kg 1kg 98% 1Ton Henan Aochuang Chemical Co.,Ltd.
5-Fluoro-2-methylaniline pictures 2022-02-19 5-Fluoro-2-methylaniline
367-29-3
US $0.00 / KG 1KG 97.4% 100 tons Honest Joy Holdings Limited
4-Fluoro-2-Aminotoluene Fluoromethylaniline7 5-Fluoro-2-methylaniline,98+% 5-Fluoro-2-methylaniline 98% 5-Fluoro-o-toluidine (NH2=1) 5-Fluoro-2-toluidine 5-Fluoro-2-methylaniline,99% 5-Fluoro-2-methylaniline,2-Amino-4-fluorotoluene, 5-Fluoro-o-toluidine 5-Fluoro-2-methylani 5-Fluoro-2-Methyl-phenylaMine Benzenamine, 5-fluoro-2-methyl- 5-FLUORO-2-METHYLANILINE 5-FLUORO-O-TOLUIDINE 3-FLUORO-6-METHYLANILINE 2 - aMino - 4 - fluorine toluene TIMTEC-BB SBB004266 5-Fluoro-2-methylaniline> 2-Amino-4-fluorotoluene~5-Fluoro-o-toluidine 2-AMINO-4-FLUOROTOLUENE 2-METHYL-5-FLUOROANILINE 367-29-3 327-29-3 Nitrogen Compounds Organic Building Blocks C7 Building Blocks Amines Miscellaneous Halogen toluene Aniline Fluorobenzene Aromatic Hydrocarbons (substituted) & Derivatives Anilines, Aromatic Amines and Nitro Compounds