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ChemicalBook >> CAS DataBase List >>3-Nitroacetophenone

3-Nitroacetophenone

CAS No.
121-89-1
Chemical Name:
3-Nitroacetophenone
Synonyms
1-(3-NITROPHENYL)ETHANONE;M-NITROACETOPHENONE;(3-nitrophenyl)methylketone;usafma-1;USAF ma-1;AKOS 233-65;AURORA 14018;3-Nitroacetofenon;AKOS BBS-00003220;3-NITROACETOPHENONE
CBNumber:
CB4400448
Molecular Formula:
C8H7NO3
Molecular Weight:
165.15
MDL Number:
MFCD00007259
MOL File:
121-89-1.mol
MSDS File:
SDS
Last updated:2024-12-18 14:08:57

3-Nitroacetophenone Properties

Melting point 76-78 °C(lit.)
Boiling point 202 °C(lit.)
Density 1.3450 (rough estimate)
vapor pressure 0.32Pa at 25℃
refractive index 1.5468 (estimate)
Flash point 202°C
storage temp. Sealed in dry,Room Temperature
solubility DMSO (Slightly), Methanol (Slightly)
form Crystalline Powder
color Yellow to yellow-green
Odor Odorless
Water Solubility <0.01 g/100 mL at 20 ºC
BRN 743002
Stability Stable. Incompatible with strong oxidizing agents, strong bases.
InChIKey ARKIFHPFTHVKDT-UHFFFAOYSA-N
LogP 1.42
EWG's Food Scores 1
FDA UNII SU4B5T763F
NIST Chemistry Reference 3-Nitroacetophenone(121-89-1)
EPA Substance Registry System 3-Nitroacetophenone (121-89-1)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H332-H335
Precautionary statements  P261-P280-P305+P351+P338
Hazard Codes  Xn
Risk Statements  21
Safety Statements  22-24/25
WGK Germany  2
RTECS  AM9625000
TSCA  Yes
HS Code  29147090
Hazardous Substances Data 121-89-1(Hazardous Substances Data)
Toxicity mouse,LD50,intraperitoneal,200mg/kg (200mg/kg),National Technical Information Service. Vol. AD277-689,
NFPA 704
1
0 0

3-Nitroacetophenone price More Price(36)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 72610 3′-Nitroacetophenone purum, ≥98.0% (GC) 121-89-1 100g $35.5 2024-03-01 Buy
TCI Chemical N0109 3'-Nitroacetophenone >98.0%(GC) 121-89-1 25g $25 2024-03-01 Buy
TCI Chemical N0109 3'-Nitroacetophenone >98.0%(GC) 121-89-1 100g $57 2024-03-01 Buy
Alfa Aesar A12155 3'-Nitroacetophenone, 98+% 121-89-1 250g $71.65 2024-03-01 Buy
Alfa Aesar A12155 3'-Nitroacetophenone, 98+% 121-89-1 500g $122.65 2024-03-01 Buy
Product number Packaging Price Buy
72610 100g $35.5 Buy
N0109 25g $25 Buy
N0109 100g $57 Buy
A12155 250g $71.65 Buy
A12155 500g $122.65 Buy

3-Nitroacetophenone Chemical Properties,Uses,Production

Chemical Properties

white to light beige crystalline powder or yellow needle-like crystals. soluble in hot water and ether, slightly soluble in ethanol. can be volatile with water vapor.

Uses

3′-Nitroacetophenone can undergo high hydrostatic pressure-assisted reduction with Ni–Al alloy in water to form 1-(3-aminophenyl)ethanol.

Uses

3''-Nitroacetophenone is used as a reactant in the synthesis of fluorine based aminothiazoles with antimicrobial activity.

Preparation

3-Nitroacetophenone is synthesized from acetophenone by nitration.
Synthesis of 3-nitroacetophenone

Production Methods

Acetophenone is carefully dissolved in concentrated sulfuric acid at 0 ℃, and mixed acid is added slowly below 0 ℃. The crude product is precipitated by quenching into ice, filtered, and washed acid free. Purification, mainly from the ortho isomer, is achieved by recrystallization from ethanol with significant lowering of the overall yield to ca. 55 %.

General Description

3-nitroacetophenone is a light beige powder. It is an anthropogenic compound which is used as a synthetic intermediate in the production of dyes and other organic compounds. (NTP, 1992)

Air & Water Reactions

Insoluble in water.

Reactivity Profile

A nitrated ketone. Ketones are reactive with many acids and bases liberating heat and flammable gases (e.g., H2). The amount of heat may be sufficient to start a fire in the unreacted portion of the ketone. Ketones react with reducing agents such as hydrides, alkali metals, and nitrides to produce flammable gas (H2) and heat. Ketones are incompatible with isocyanates, aldehydes, cyanides, peroxides, and anhydrides. They react violently with aldehydes, HNO3, HNO3 + H2O2, and HClO4.

Fire Hazard

Flash point data for 3-Nitroacetophenone are not available, however 3-Nitroacetophenone is probably combustible.

Purification Methods

Distil the ketone in steam and crystallise it from EtOH. [Beilstein 7 IV 656.]

Global( 494)Suppliers
Supplier Tel Email Country ProdList Advantage
Hebei Yanxi Chemical Co., Ltd. 		+8617531190177 peter@yan-xi.com China 5857 58
Hebei Chuanghai Biotechnology Co,.LTD 		+86-13131129325 sales1@chuanghaibio.com China 5889 58
Hebei Weibang Biotechnology Co., Ltd 		+8617732866630 bess@weibangbio.com China 18151 58
Henan Fengda Chemical Co., Ltd 		+86-371-86557731 +86-13613820652 info@fdachem.com China 20284 58
airuikechemical co., ltd. 		+undefined86-15315557071 sales02@sdzhonghuimaterial.com China 983 58
Capot Chemical Co.,Ltd. 		+86-（0）57185586718 +86-13336195806 sales@capot.com China 29791 60
Beijing Cooperate Pharmaceutical Co.,Ltd 		010-60279497 sales01@cooperate-pharm.com CHINA 1803 55
Henan Tianfu Chemical Co.,Ltd. 		+86-0371-55170693 +86-19937530512 info@tianfuchem.com China 21634 55
Tianjin Zhongxin Chemtech Co., Ltd. 		+86-022-66880623 +8618622897568 sales@tjzxchem.com China 563 58
Shanxi Naipu Import and Export Co.,Ltd 		+86-13734021967 +8613734021967 kaia@neputrading.com China 1001 58

View Lastest Price from 3-Nitroacetophenone manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
3-Nitroacetophenone pictures 2024-10-25 3-Nitroacetophenone
121-89-1
 US $0.00 / kg 1kg 0.99 20 tons Hebei Yanxi Chemical Co., Ltd.
3-Nitroacetophenone pictures 2024-10-25 3-Nitroacetophenone
121-89-1
 US $0.00-0.00 / KG 50KG 99% 500000kg Hebei Weibang Biotechnology Co., Ltd
3-nitroacetophenone pictures 2024-10-15 3-nitroacetophenone
121-89-1
 US $0.00-0.00 / Kg 1Kg 99.9% 200tons airuikechemical co., ltd.
3’-nitroacetophenone[qr] 3-Nitroacetofenon Acetophenone, 3'-nitro- acetophenone,3’-nitro-[qr] Ethanone, 1-(3-nitrophenyl)- Ethanone,1-(3-nitrophenyl)- ethanone,1-(3-nitrophenyl)-[qr] m-Acetylnitrobenzene Methyl 3-nitrophenyl ketone methyl3-nitrophenylketone methyl3-nitrophenylketone[qr] USAF ma-1 3'-Nitroacetophenone Vetec(TM) reagent grade, 98% m-Nitroacetophenone 1-(3-Nitrophenyl)ethanone usafma-1 META NITRO ACETOPHENONE 6-CHLOROMETHYL-3-FORMYLCHROMONE M-Nitroacetophenone, 98% 100GR 3'-Nitroacetophenone, 98+% m-NITROACETOPHENONE pure 3-Acetyl-1-nitrobenzene m-Nitroacetophenone,98% 1-(3-Nitrophenyl)ethan-1-one, 3-Acetylnitrobenzene, 3-Ethanoylnitrobenzene Nitrobenzene between ethyl ketone 3'-Nitroacetophenone purum, >=98.0% (GC) 3'-Nitroacetophenone ReagentPlus(R), 99% 3'-NITROACETOPHENONE 3-NITROACETOPHENONE 1-Acetyl-3-nitrobenzene 3’-nitro-acetophenon (3-Nitrophenyl) methyl ketone 1-(3-nitrophenyl)-ethanon AKOS BBS-00003220 AKOS 233-65 LABOTEST-BB LT01895210 AURORA 14018 2-[[1-(3-chlorophenyl)-1,2,4-triazol-3-yl]oxy]propanamide 3'-Nitroacetophenone> 3-Nitroacetophenone ISO 9001：2015 REACH M-NITROACETOPHENONE (3-nitrophenyl)methylketone 1-(3-NITROPHENYL)ETHANONE Paracetamol Impurity 29 3-Nitroacetophenone (3NAP) 3'-nitroacetophenone 3-Nitroacetophenone 98% For Synthesis 121-89-1 KETONE Organic Building Blocks Ketones C7 to C8 Carbonyl Compounds Building Blocks Carbonyl Compounds Ketones Building Blocks C7 to C8 Carbonyl Compounds