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ChemicalBook--->CAS DataBase List--->74316-27-1

74316-27-1

74316-27-1 Structure

74316-27-1 Structure
IdentificationBack Directory
[Name]

CIS-3-AMINOCYCLOBUTANECARBOXYLIC ACID
[CAS]

74316-27-1
[Synonyms]

cis-3-Amino-cyclobutaneca...
3-aminocyclobutane-1-carboxylic acid
CIS-3-AMINOCYCLOBUTANECARBOXYLIC ACID
cis-3-aminocyclobutane-1-carboxylic acid
Cyclobutanecarboxylic acid, 3-amino-, cis-
rel-(1R,3R)-3-aMinocyclobutane-1-carboxylic acid
[Molecular Formula]

C5H9NO2
[MDL Number]

MFCD06659964
[MOL File]

74316-27-1.mol
[Molecular Weight]

115.13
Chemical PropertiesBack Directory
[storage temp. ]

Keep in dark place,Inert atmosphere,Room temperature
Safety DataBack Directory
[Symbol(GHS) ]


GHS07
[Signal word ]

Warning
[Hazard statements ]

H335-H319-H315
[Precautionary statements ]

P264-P280-P305+P351+P338-P337+P313P-P264-P280-P302+P352-P321-P332+P313-P362
[Hazard Codes ]

Xi
[Hazard Note ]

Irritant
Hazard InformationBack Directory
[Uses]

CIS-3-AMINOCYCLOBUTANECARBOXYLIC ACID can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
[Synthesis]

 1.png
Azide 10a (0.30 g, 1.9 mmol) was dissolved in methanol (5 mL); then 6N HCl (2 mL) and 10% palladium on charcoal were added to the solution. The resulting mixture was stirred under 1 bar of hydrogen for 3 h, then the catalyst was filtered off, and the solvent was removed under reduced pressure. The residue was dissolvedin 6N HCl (5 mL) and refluxed upon stirring for 1 h, then evaporated in vacuum. The residue was purified by ion-exchange chromatography (Amberlite? IR-120(plus) ion-exchange resin, 3.5% aqueous ammonia as an eluent). cis-3-aminocyclobutanecarboxylic acid 1a as white powder, yield 0.16 g, 1.4 mmol, 71%.
Spectrum DetailBack Directory
[Spectrum Detail]

CIS-3-AMINOCYCLOBUTANECARBOXYLIC ACID(74316-27-1)1HNMR
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