Identification | Back Directory | [Name]
1-ADAMANTYLOXYCARBONYL FLUORIDE | [CAS]
62087-82-5 | [Synonyms]
ADOC-F 1-ADOC-F ADAMANTYL FLUOROFORMATE 1-ADAMANTYL FLUOROFORMATE 1-ADAMANTYLOXYCARBONYL FLUORIDE 1-ADAMANTYL FLUOROFORMATE, 90+% Adamantan-1-yl carbonofluoridate 1-Adamantyl carbonofluoridic acid Fluoroformic acid adamantan-1-yl ester Fluoridocarbonic acid 1-adamantyl ester (tricyclo(3,3,1,1,3,7)decan-1-yl) fluoroformate Fluoroformic acid tricyclo[3.3.1.13,7]decan-1-yl ester Carbonofluoridic acid,tricyclo[3.3.1.13,7]dec-1-yl ester | [EINECS(EC#)]
263-400-6 | [Molecular Formula]
C11H15FO2 | [MDL Number]
MFCD00074772 | [MOL File]
62087-82-5.mol | [Molecular Weight]
198.23 |
Hazard Information | Back Directory | [Purification Methods]
Dissolve it in n-hexane (ca 10g in 150 mL) and keep at 0o for 24hours. Any 1-adamantanol present will separate. Filter and evaporate to dryness. The crystalline residue has m 31-32o and is recrystallised from n-hexane (90g/500mL), (IR (KBr): max 1242, 1824 and 2340 cm-1). There should be no OH str band above 2500 cm-1. [Moroder et al. Hoppe-Seyler’s Z Physiol Chem 357 1647 1976, cf Haas et al. J Am Chem Soc 88 1988 1966.] |
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