Identification | Back Directory | [Name]
3,4-Dichloro-4'-hydroxybenzophenone | [CAS]
60013-02-7 | [Synonyms]
Fenofibrate impurity 5 Fenofibrate Impurity 14 3,4-Dichloro-4'-hydroxybenzophenone 3,4-dichlorophenyl 4-hydroxyphenyl ketone (3,4-Dichlorophenyl)(4-hydroxyphenyl)methanone Methanone, (3,4-dichlorophenyl)(4-hydroxyphenyl)- | [Molecular Formula]
C13H8Cl2O2 | [MOL File]
60013-02-7.mol | [Molecular Weight]
267.11 |
Hazard Information | Back Directory | [Preparation]
Preparation by reaction of 3,4-dichlorobenzoyl chloride, ? with phenol in the presence of aluminium chloride; ? with phenetole in the presence of aluminium chloride in carbon disulfide at r.t. overnight (40%); ? with anisole in the presence of aluminium chloride at 70° for 4 h, followed by demethylation of the obtained ketone with 48% hydrobromic acid in refluxing acetic acid for 47 h. |
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